[1]陈林,刘立峰,李珍,等.不同埋烧氛围BNKT5陶瓷的结构与性能[J].武汉工程大学学报,2009,(12):59-62.
CHEN Lin,LIU Li feng,LI Zhen,et al.Structure and properties of BNKT5 ceramics prepared under different atmosphere of burying sintering[J].Journal of Wuhan Institute of Technology,2009,(12):59-62.
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不同埋烧氛围BNKT5陶瓷的结构与性能(
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]
- 卷:
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- 期数:
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2009年12期
- 页码:
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59-62
- 栏目:
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材料科学与工程
- 出版日期:
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2009-12-28
文章信息/Info
- Title:
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Structure and properties of BNKT5 ceramics prepared under
different atmosphere of burying sintering
- 文章编号:
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16742869(2009)12005904
- 作者:
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陈林1; 2; 刘立峰1; 2; 李珍1; 2; 杜城1; 2; 林少亮1; 2
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1.教育部纳米矿物材料及应用工程研究中心,中国地质大学,湖北 武汉 430074;
2.中国地质大学(武汉)材料科学与化学工程学院,湖北 武汉 430074
- Author(s):
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CHEN Lin1; 2; LIU Lifeng1; 2; LI Zhen1; 2; DU Cheng1; 2; LIN Shaoliang1; 2
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1. Engineering Research Center of NanoGeomaterials of Ministry of Education, China University of Geosciences,
Wuhan 430074, China; 2. Faculty of Material Science and Chemical Engineering, China University of Geosciences,
Wuhan 430074, China
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- 关键词:
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BNKT; 柠檬酸盐法; 埋烧; 压电陶瓷
- Keywords:
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BNKT; citrate method; burying sintering; piezoelectric ceramics
- 分类号:
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TM282
- DOI:
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- 文献标志码:
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A
- 摘要:
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采用柠檬酸盐法制备出Bi0.5(Na0.95K0.05)0.5TiO3(BNKT5)无铅压电陶瓷,通过XRD、SEM等测试手段,研究了BNKT5粉体合成温度及陶瓷埋烧氛围对BNKT5陶瓷性能与结构的影响.结果表明,烧结温度为1 130 ℃时,利用750 ℃合成BNKT5粉体,在Al2O3粉中埋烧制备的BNKT5陶瓷的晶粒结晶度高,呈紧密堆积,大小分布均匀,具有较高的压电常数、机械品质因数和较低的介电损耗.
- Abstract:
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The leadfree Bi0.5(Na0.95K0.05)0.5TiO3 (BNKT5) piezoelectric ceramics were prepared by citrate method. Their structure and properties were determined by using Xray diffraction and scanning electron microscope, respectively. The effects of calcining temperature for BNKT5 powder and atmosphere of burying sintering for BNKT5 ceramics on the structure and properties have been investigated. This study indicated that the calcining temperature 750 ℃ for the BNKT5 powder and 1 130 ℃ in Al2O3 for the ceramics are needed for the BNKT5 ceramics, which possesses packing density of grain, uniform grain in size, good crystallinity and hence higher piezoelectric constant, mechanical quality factor and lower dielectric loss in this work.
参考文献/References:
[1]李月明,陈文,江向平,等. Na0.5Bi0.5TiO3K0.5Bi0.5TiO3系无铅压电陶瓷的极化工艺研究[J]. 中国陶瓷,2006,7(42): 1720.
[2]喻德忠,艾军,邹菁. 纳米级金属氧化物的合成及其性质比较[J]. 武汉工程大学学报,2007,3(29): 13.
[3]廖润华,李月明,江向平,等. 溶胶—凝胶法制备Na0.5Bi0.5TiO3K0.5Bi0.5TiO3 体系无铅压电陶瓷的研究[J]. 人工晶体学报,2008,3(37): 652655.
[4]王孝平,赁敦敏,廖运文,等. Bi0.5 (Na0.85K0.15)0.5TiO3压电陶瓷溶胶—凝胶法制备技术研究[J]. 四川大学学报(自然科学版),2005,2(42): 464467.
[5]Qing Xu,Shutao Chen,Wen Chen,et al. Synthesis and piezoelectric and ferroelectric properties of (Na0.5Bi0.5)1xBaxTiO3 ceramics[J]. Materials Chemistry and Physics,2005(90): 111115.
[6]廖运文,赁敦敏,肖定全,等. 钛酸铋钠钾锂无铅陶瓷的柠檬酸制备技术[J]. 无机盐工业,2006,2(38): 1921.
[7]陈书涛,徐庆,陈文,等. (Na0.5Bi0.5)TiO3BaTiO3的合成与压电性能[J]. 材料研究学报,2004,5(18): 524528.
[8]徐寿昌. 有机化学[M]. 北京: 高等教育出版社,1982: 313.
备注/Memo
- 备注/Memo:
-
收稿日期:20090708
作者简介:陈林(1983),男,河南驻马店人,硕士研究生.研究方向:压电陶瓷的制备与表征.
作者简介:李珍,女,博士,教授,博士生导师.研究方向:岩石矿物材料学,材料学.
更新日期/Last Update: