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[1]陈凡,刘永红,刘永琼*,等.番石榴果芳香浸膏的提取及成分分析[J].武汉工程大学学报,2010,(12):13-17.[doi:10.3969/j.issn.16742869.2010.12.004]
 CHEN Fan,LIU Yong hong,LIU Yong qiong,et al.Extract and analysis Aroma Extract of Guava Fruit [J].Journal of Wuhan Institute of Technology,2010,(12):13-17.[doi:10.3969/j.issn.16742869.2010.12.004]
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番石榴果芳香浸膏的提取及成分分析
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2010年12期
页码:
13-17
栏目:
资源与土木工程
出版日期:
2010-12-31

文章信息/Info

Title:
Extract and analysis Aroma Extract of Guava Fruit
文章编号:
16742869(2010)12001305
作者:
陈凡1刘永红2刘永琼1*李亮1陈雅芬1黎璐平1
1.武汉工程大学化工与制药学院,绿色化工过程省部共建教育部重点实验室,
新型反应器与绿色化学工艺湖北省重点实验室,湖北 武汉 430074;
2.襄樊市中心医院, 湖北 襄樊 441021
Author(s):
CHEN Fan1 LIU Yonghong2 LIU Yongqiong1 CHEN Yafen1 LI Liang1 LI Luping1
1.School of Chemical Engineering & Pharmacy, Wuhan Institute of Technology,
Key Laboratory for Green Chemical Process of Ministry of Education, Hubei Key Laboratory of
Novel Chemical Reactor & Green Chemical Technology, Wuhan 430074, China;
2.Xiangfan Central Hospital, Xiangfan 441021, China
关键词:
番石榴果芳香浸膏提取正交设计GCMS
Keywords:
guava fruit aromatic extract extraction orthogonal design GCMS
分类号:
R284.1
DOI:
10.3969/j.issn.16742869.2010.12.004
文献标志码:
A
摘要:
采用乙醇作溶媒对番石榴果进行芳香浸膏的提取,通过小试及正交设计得出最佳工艺为物料比15、温度40 ℃、提取3 h,此时乙醇质量分数为80%,浸膏得率可达22.6%.并采用GCMS联用技术对提取所得芳香浸膏进行成分分析,可能的成分及质量分数为:5羟甲基糠醛(71.47%)、2,32H3,5二羟基6甲基4H吡喃酮(6.44%)、糠醛(4.69%)、乙酸(2.54%)、庚酸(1.70%)等.
Abstract:
Using ethanol as solvent to extract the aromatic extract from guava fruit , we got the best technology by small scales and orthogonal design: the material ratio was 15, the temperature was 40 ℃, extraction time was 3 hours, 80 % ethanol,extract yield was 22.6%. The authors analyzed the composition of the extract by GCMS spectrometry technique, and obtained the main components which were:5hydroxymethyl furfural (71.47%) and 2,3dihydro3,5di hydroxy6methyl4HPyran4one (6.44%), furfural (4.69%), acetic acid (2.54%), Heptanoic acid (1.70%), etc.

参考文献/References:

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[8]国家标准化管理委员会.水果、蔬菜产品中干物质和水分含量的测定方法[S].中国人名共和国商业部,1988:14.
[9]鄢文,周迎春,刘强,等.正交实验法优选番石榴叶挥发油提取工艺[J].中国实验方剂学杂志,2008,14(6):2526.
[10]杨靖,黎莉,戴立珍,等.白玉兰种子挥发油成分的GCMS分析[J].武汉工程大学学报,2010,32(3):4748.

相似文献/References:

[1]刘永琼,余佩,陈雅芬,等.菠萝蜜芳香浸膏的质量标准[J].武汉工程大学学报,2013,(08):19.[doi:103969/jissn16742869201308004]
 LIU Yong qiong,YU Pei,CHEN Ya fen,et al.Quality standard of jackfruit aromatic extract[J].Journal of Wuhan Institute of Technology,2013,(12):19.[doi:103969/jissn16742869201308004]

备注/Memo

备注/Memo:
收稿日期:20100903作者简介:陈凡(1985),女,湖北黄冈人,硕士研究生.研究方向:天然产(药)物的研究与开发.指导老师:刘永琼,女,教授,硕士研究生导师.研究方向:药物合成、药物制剂与天然药物.
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