|本期目录/Table of Contents|

[1]徐秀廷,赵玉英*,顾德昌.气相色谱法分析蒙药白头翁多糖的单糖组分[J].武汉工程大学学报,2011,(07):31-33.
　XU Xiu ting,ZHAO Yu ying,GU De chang.Component analysis of monosaccharide in polysaccharides for Mongolian Medicine Pulsatilla chinensis by gas chromatography[J].Journal of Wuhan Institute of Technology,2011,(07):31-33.
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2011年07期
页码:
31-33
栏目:
材料科学与工程
出版日期:
2011-08-30

文章信息/Info

Title:
Component analysis of monosaccharide in polysaccharides for
Mongolian Medicine Pulsatilla chinensis by gas chromatography
文章编号:
16742869(2011)07003103
作者:
徐秀廷1; 赵玉英2*; 顾德昌1
1. 内蒙古民族大学化学化工学院，內蒙古 通辽 028043；
2. 内蒙古民族大学分析测试中心，內蒙古 通辽 028043
Author(s):
XU Xiuting1;  ZHAO Yuying2;  GU Dechang1
1.College of Chemical Technology, Inner Mongolia Universit for Nationalities, Tongliao 028043, China;
2.Center of Analysis and Test, Inner Mongolia University for Nationalities, Tongliao 028043, China
关键词:
白头翁; 气相色谱; 多糖
Keywords:
Mongolian Medicine Pulsatilla chinensis;  gas phase chromatography;  polysaccharide
分类号:
O657.7+1
DOI:
-
文献标志码:
AAdoi:10.3969/j.issn.16742869.2011.07.009
摘要:
将白头翁多糖经水解和乙酰化处理，采用气相色谱法分析多糖中单糖组分，得到白头翁多糖的单糖组分，白头翁多糖的单糖组分及摩尔比为M鼠李糖M阿拉伯糖M木糖M甘露糖M半乳糖M葡萄糖=10.222.340.451282.411.82.气相色谱条件：色谱柱为Thermo TR-5ms，程序升温100 ℃10 ℃/min150 ℃5 ℃/min260 ℃、进样量为１ μL，此检测方法用标准样品的积分面积和内标法分别进行了定量，内标物肌醇的标准曲线回归方程为Y=0.446X+0.057 5（r=0.999 0），回收率为103.04%，RSD为0.39%.
Abstract:
The GC analysis was used to study the monosaccharide composition of polysaccharide in Pulsatilla chinensis polysaccharide after hydrolyzing and acetylation. The monosaccharide components and the molar ratio is MrhamnoseMarabinoseMxyloseMinositolMmannoseMglucose=10.222340.451.282.41182. Gas chromatography conditions are as follow: column for the Thermo TR-5ms, temperature-programmed to 100 ℃ and then 260 ℃, the injection amount of 1 μL. We used the peak area of standard samples and internal standard curve method to analyze these monosaccharides, respectively. The linear regression equation was Y=0.446X+0.057 5（r=0.999 0）, recovery was 10304%, and RSD was 0.39%.

参考文献/References:

［1］张晓琦，石宝俊，李药兰，等.白头翁地上部分的化学成分研究［J］.中草药，2005，39（5）：651653
［2］ 陈凡,刘永红,刘永琼,等,番石榴果芳香浸膏的提取及成分分析［J］.武汉工程大学学报,2010，32(12):1317
［3］ 周霁，向建敏.高效液相色谱法测定多溴联苯醚含量的研究［J］.武汉工程大学学报，2008，30（3）：1821
［4］ 周峰，杨建设，杨艺虹，等.紫外分光光度法测定瑞巴匹特颗粒剂含量［J］.武汉工程大学学报,2007,29(1):1012
［5］ 方艳夕,晏明炉,秦梅颂,等.不同炮制方法对白头翁多糖含量的影响［J］. 中兽医医药杂志，2010（3）：1416

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